Hi everybody. I have a green palladium solution. I took a sample of it and I added a DMG and sodium hydroxide solution to the green pd solution. It precipitated green powder. I read in some forums that I should filtrate the powder and wash it with cold water until it gets yellow pdDMG powder. When I washed it it got white color. Am I doing something wronge? Or I didnt make the DMG solution correctly. I tested the green solution with Stannous chloride before and after adding DMG solution. Before it was positive after adding it got negative with the green precipitate. What should I do?
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Hello! It sounds like you're working through a complex refining process, and it's understandable to encounter some surprises along the way. When dealing with palladium refining and the formation of PdDMG, variations in color can sometimes be caused by impurities or incomplete reactions. Double-check your DMG solution preparation to ensure it's at the correct concentration, and make sure your washing process is thorough but gentle to avoid removing any residual palladium. Also, testing with Stannous chloride is a good step—if the test turns negative after adding DMG, it might indicate the palladium is precipitated and removed as expected. As a fun side note, just like how you’re refining precious metals, I’ve been experimenting with different makeup looks using Maybelline Products—sometimes a little trial and error leads to the best results!
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Using DMG for palladium precipitation can be effective, but purity depends heavily on pH control and prior filtration. Just like finding quality gear at the right goodwill outlet store locations – goodwill outlets, refining success is all about knowing where and how to source properly.
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Palladium refining with DMG involves dissolving the metal in solution, Spotify Mod APK then using dimethylglyoxime to selectively precipitate it as a red-brown complex. This method requires careful pH control and clean separation from other metals. The precipitate is filtered, washed, and reduced to recover pure palladium in metallic form.
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Palladium refining with DMG involves using Dimethylglyoxime as a reagent to selectively extract and purify palladium from mixtures. This process is important in precious metal recovery and recycling. For more detailed explanations on such chemical techniques and related tech, the Profit Techy site provides clear, easy-to-understand guides.
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It sounds like you're on the right track with palladium refining using DMG (Dimethylglyoxime), but the color change could indicate incomplete washing or impurities in the process. The green precipitate suggests a palladium-DMG complex, but if it turns white instead of yellow, you might not be washing thoroughly or your DMG solution concentration may be off. Ensure you're using the correct pH and washing with very cold water. Also, verifying your DMG purity and process consistency is crucial. Just like refining palladium requires precision, getting the best gaming experience often requires the right resources—if you're into simulation games, Truck Simulator Ultimate Mod APK Unlimited Money and Gold can enhance your gameplay significantly!
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düşük ısıda buharlaştır.yoğunlaşmış paladyumklor elde et.paladyumklorun içinden klor gazı geçer.paladyum tuzu çöker. klor gazı geçince çökmemişse,ortamda ya od yoktur,ya da PdCl2 yoğunlaştırılmamıştır.
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hello everyone i hope you all have a good day. i got into a big mess here, i scraped hundreds of cell phones, remove as much plastic as possible and also removed iron from it but still there is a big quantity of base metals, i burned everything for the acid to do a good job and i ended up with a half 5 gallon bucket full of copper mixed with all kind of metals from cell phones and computers in total is about 5 kilos of mixed boards
tried to separate every component manually because there is a considerable amount of palladium since most of the boards are from phones, ipads and computers but i found out is very difficult
there are all kind of mixed metals so i just added concentrated nitric acid to get first the copper, im new in this so i wonder if adding the acid was the right thing to do, there are many ics that neeed to be crush i think i made a mistake, please help
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same to you my halp
Okay
Re-dissolve with water/dilute HCl and add the copper
So what could I do if the precipitate has the pd?
Ok I already did that and I will let it for some days. But what if the precipitate do contain pd in it and there is no in the solution? Should I do tue SMB process?
Yes and what do yoy advice me to do?
Hi I made a 20ml DMG solution with 2grams DMG with 20ml water and I added like 15ml to the solution. Here is the precipitate I got. One friend told me to dissolve this precipitate in nitric acid and then dilute the solution and add SMB and a yellow palladuim precipitate will settpe but I am not sute should I do that?
Hi,
It sounds like you may have precipitated some hydoxides / oxides.
How much. DMG solution have you added? Is the leach solution still acidic?